Rapid and Mild Cleavage of Aryl‐Alkyl Ethers to Liberate Phenols

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We report that the Piers-Rubinsztajn reaction permits quick deprotection of aryl alkyl ethers below ambient circumstances. This chemistry leverages tris(pentafluorophenyl)borane and silyl hydrides to transform aryl methyl ethers to siloxanes, which can then be cleaved working with

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